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Journal of Microscopy

Publication date: 2006-12-01
Volume: 224 Pages: 256 - 263
Publisher: Blackwell Science

Author:

Walentek, Artur
Seefeldt, Marc ; Verlinden, Bert ; Aernoudt, Etienne ; Van Houtte, Paul

Keywords:

electron backscatter diffraction, pearlite, pearlite colony, growth, Science & Technology, Technology, Microscopy, GROWTH, 0204 Condensed Matter Physics, 0601 Biochemistry and Cell Biology, 0912 Materials Engineering, 3101 Biochemistry and cell biology, 3406 Physical chemistry, 4016 Materials engineering

Abstract:

Electron backscatter diffraction measurements were performed on a set of pearlitic steel samples after different heat treatments. The strengths and limitations of the technique with respect to the pearlite issue are presented. Interpretation of the obtained results confirmed that more than one pearlite colony may exist inside one ferrite nodule of nearly the same crystallographic orientation. It was also found that, in most cases, a misorientation of the order of several degrees exists between pearlite colonies within one ferrite nodule. Moreover, the ferrite matrix exhibits changes of crystallographic orientation inside colonies often accompanied by a network of low angle boundaries. The mean size of the ferrite nodule in the matrix was determined by means of electron backscatter diffraction. However, determination of the mean pearlite colony size was difficult and often impossible by means of both metallographic methods and electron backscatter diffraction measurements.