Title: Hadamard 1D H-1 TOCSY and its application to oligosaccharides
Authors: Schraml, Jan ×
van Halbeek, H
De Bruyn, André
Contreras, R
Maras, M
Herdewijn, Piet #
Issue Date: Dec-1997
Publisher: John wiley & sons ltd
Series Title: Magnetic resonance in chemistry vol:35 issue:12 pages:883-888
Abstract: Replacement of a series of N consecutive one-site selective excitation NMR experiments by N simultaneous N-site excitations with phases of component pulses varied according to the N x N Hadamard matrix offers a sensitivity improvement of the order of root N (for N = 2, 4, 8,..,) [R. Freeman, Spin Choreography, pp. 177-183. Spektrum, Oxford (1996)]. Here this principle was extended to one-dimensional (1D) H-1 TOCSY experiments, in the absence and presence of heteronuclear decoupling, The 1D H-1 Hadamard TOCSY technique was applied to selected oligosaccharides, representing a class of biomolecules for which multiple 1D TOCSY experiments are the mainstay in H-1 NMR spectral assignment and structural characterization. (C) 1997 John Wiley & Sons, Ltd.
ISSN: 0749-1581
Publication status: published
KU Leuven publication type: IT
Appears in Collections:Medicinal Chemistry (Rega Institute)
× corresponding author
# (joint) last author

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