Title: Quantitative determination of olaquindox in animal feed
Authors: Roets, Eugene ×
Quintens, Ivo
Kibaya, R
Hoogmartens, Jos #
Issue Date: Sep-2001
Publisher: Research inst medicinal plants
Series Title: Jpc-journal of planar chromatography-modern tlc vol:14 issue:5 pages:347-349
Abstract: A quantitative thin layer chromatographic (TLC) method on silica gel, with ethyl acetate-acetone-alcohol, 62 + 40 + 3 (v/v) as mobile phase, has been developed for the determination of olaquindox at ppm levels in animal feed. Preliminary purification consists of extraction with water, adsorption on XAD-4, washing, and elution with acetonitrile. Before the ellution step acetylolaquindox is added as internal standard. The residue obtained after evaporation of acetonitrile is dissolved in a small volume of methanol. Quantitation is performed by densitometry at lambda = 360 nm.
ISSN: 0933-4173
Publication status: published
KU Leuven publication type: IT
Appears in Collections:Pharmaceutical Analysis
× corresponding author
# (joint) last author

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