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Title: Collaborative study of the analysis of tylosin by liquid chromatography on wide-pore poly(styrene-divinylbenzene)
Authors: Paesen, J ×
Crommen, J
Debeer, J
Jin, Sh
Porqueras, E
Vanoverbeke, A
Violon, C
Hoogmartens, Jos #
Issue Date: 1995
Publisher: Marcel dekker inc
Series Title: Journal of liquid chromatography vol:18 issue:6 pages:1195-1205
Abstract: A previously developed method for analysis of tylosin A and related substances by liquid chromatography using a wide-pore poly(styrene-divinylbenzene) stationary phase was examined in a multicentre study involving 7 laboratories and 3 samples. The main component and the impurities were determined. An analysis of variance showed absence of consistent laboratory bias and significant laboratory-sample interaction at the 1 % level. Estimates for the repeatability and reproducibility of the method, expressed as standard deviation (SD) of the result of the determination of tylosin A, were calculated to be 1.3 % and 1.6 % respectively.
ISSN: 0148-3919
Publication status: published
KU Leuven publication type: IT
Appears in Collections:Pharmaceutical Analysis
× corresponding author
# (joint) last author

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