Title: An improved gas chromatographic assay for spectinomycin hydrochloride
Authors: Hoebus, J ×
Yun, Li Ming
Hoogmartens, Jos #
Issue Date: Jul-1994
Publisher: Friedr vieweg sohn verlag gmbh
Series Title: Chromatographia vol:39 issue:1-2 pages:71-73
Abstract: A gas chromatographic assay for spectinomycin hydrochloride is described. The method is based on that prescribed by the United States Pharmacopeia (USP XXII). The method involves silylation of spectinomycin hydrochloride; phenazone is used as an internal standard. Spectinomycin and phenazone have adequate stability under the prescribed conditions. The stationary phase is 3 % OV-17 on Gaschrom Q 100-120 mesh. The selectivity of the proposed method is better than that of the GLC method described in the USP XXII.
ISSN: 0009-5893
Publication status: published
KU Leuven publication type: IT
Appears in Collections:Pharmaceutical Analysis
× corresponding author
# (joint) last author

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