Title: Characterisation of reversed-phase liquid chromatographic columns by chromatographic tests. Evaluation of 36 test parameters: repeatability, reproducibility and correlation
Authors: Visky, Dóra ×
Vander Heyden, Yvan
Iványi, Tímea
Baten, Peggy
De Beer, Jacques
Kovács, Zsuzsanna
Noszál, Béla
Roets, Eugene
Massart, Désiré L
Hoogmartens, Jos #
Issue Date: Nov-2002
Series Title: Journal of Chromatography A vol:977 issue:1 pages:39-58
Abstract: The European Pharmacopoeia (Ph. Eur.) or other official compendia give only a general description of the stationary phase in the description of a liquid chromatographic method. Therefore the selection of a column giving suitable selectivity presents difficulties. Earlier, a test procedure was proposed that allows measurement of a number of parameters which are reported to be representative for stationary phase characteristics. This paper describes how the test procedure was applied on 69 RP-LC C18 columns. Chromatographic parameters obtained as test results were evaluated, and their repeatability, reproducibility and correlation were examined.
ISSN: 0021-9673
Publication status: published
KU Leuven publication type: IT
Appears in Collections:Pharmaceutical Analysis
× corresponding author
# (joint) last author

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